The 6400 Automatic Isoperibol Calorimeter represents the next evolutionary step in the Parr automated calorimeters. Inclusive and compact, the instrument incorporates a closed loop cooling subsystem into the calorimeter. This subsystem uses a thermoelectric cooler assembly attached directly to a one liter water tank which supplies cooling water to the calorimeter. An external nitrogen pressurized tank is used to supply rinse water to the calorimeter. This model features the fixed bomb and bucket design allowing for automated bucket and jacket fill as well as automated vessel fill and rinse. The 6400 requires one minute of operator time per test, allowing a technician to operate up to four calorimeters simultaneously.
Design Features
Parr Fixed Bomb and Bucket Technology
The 6400 Automatic Isoperibol Calorimeter uses a fixed bomb and bucket design where the bomb and bucket are not removed from the calorimeter during routine operations. This design concept has made it possible to offer unique levels of automation for the entire calorimetric determination not just the data collection and reporting steps. The result of this automation will save approximately five minutes of operator time per test when compared to any removable bomb calorimeter.
Oxygen Charging and Release
The fixed bomb and bucket design allow the oxygen supply to be directed into the head of the bomb at the beginning of each test. The head of these bombs incorporate a check valve which dynamically seals when the bomb is pressurized. At the end of the test, the gases in the bomb are automatically released while the calorimeter is being returned to its starting temperature.
Fixed Bucket
The bucket in these calorimeters has been designed to provide smooth circulation over the surface of the vessel. The design also repeatedly fills the bucket volumetrically. The bomb head closure seals the bucket at the same time the bomb is closed. This unique design minimizes the amount of water required for the test as well as permitting rapid, automatic and repeatable filling for each test. The water heated by the combustion is automatically drained from the bucket at the conclusion of the test and replaced with cooling water to bring the bomb and bucket rapidly back down to the starting temperature for the next test.
Fixed Bomb
The 6400 Calorimeter features the patented closure design of the Parr Fixed bombs. This design allows the user to seal and lock the head into the cylinder with simple one sixteenth turn. The main bomb seal is an o-ring optimized to minimize frictional wear, improving the lifetime of this seal. At the conclusion of the test the inside surface of the bomb is washed to remove the products of the combustion from the bomb. The automation of the bomb washing step eliminates one of the most tedious and time consuming manual operations required with removable bomb calorimeters. Besides the elimination of the drudgery of manually washing the bomb, a not so obvious advantage of the fixed bomb design is that the bomb is always washed as soon as the final temperature can be determined. Generally, this is within 4-5 minutes of the time the bomb is fired. This holds to an absolute minimum the time any acids produced by the combustion can attach to the inner surfaces of the bomb. This has improved the service life of these bombs in comparison to removable bombs.
1138 Oxygen Combustion Bomb
The 1138 oxygen bomb is the standard bomb in the 6400 calorimeter. The 1138 Oxygen Bomb has been redesigned to withstand a higher magnitude of tests. The head is designed with an O-ring groove which is optimized to minimize frictional wear, in turn improving the lifetime of the seal. The bomb head is removable for fast sample loading using the patented Quick Twist-Lock vessel closure design.
The bomb is made from alloy 20; a special niobium stabilized stainless steel selected for its resistance to the mixed nitric and sulfuric acids produced during the combustion process. The 1138CL is made from the halogen resistant Hastelloy G30™. Hastelloy 30™ is an alloy rich in cobalt and molybdenum and is able to resist the corrosive effects of free chlorine and halogen acids produced when burning samples with significant chlorine content. While no alloy will completely resist the corrosive atmospheres produced when burning samples containing halogen compounds, users who intend to test these materials are urged to select the 1138CL Bomb.
These bombs are 250 mL in volume and are rated to a working pressure of 2000 psi. The bombs are hydrostatically tested to 3000 psi and the sample range is ~1g releasing up to 8000 calories per test.
A1450DD Head
Users who wish to achieve maximum through-put with their 6400 calorimeters will want to purchase a spare A1450DD head for their calorimeter. This permits the next sample to be completely prepared and inserted into the bomb as soon as the current test is concluded.
Control Charts
A control chart is a graphical tool which can assist the user in determining whether or not their process is in control. Many standard methods will dictate that a reference sample be measured periodically and the results plotted on a graph. Limits for acceptable values are defined and the process is assumed to be in control as long as the results stay within these limits. Since results are expected to scatter with a normal distribution within established limits, systematic trends or patterns in the data plots may also be an early warning of problems. The 6400 calorimeter provides the user with the ability to instantaneously plot and view standard results with user defined warning and control limits.
Laboratory Requirements
The calorimeter requires a source of 99.5% oxygen, a source of nitrogen or house air at 80 psi, and deionized water.
C 200-System consists of the following components:
Measuring cell C 200
Decomposition vessel C 5010
Oxygen filling station C 248
Consumables for calibrations and installation
Space-saving and low cost combustion calorimeter for determing gross calorific values of liquid and solid samples.
Validation according to DIN 51900,ISO 1928, ASTM D240, ASTM D4809, ASTM D5865, ASTM D1989, ASTM D5468, ASTM E711.
Suitable for teaching and training, as well (f.e tecnical- schools, universities) and for industriell laboratories with less analyses..
Manual handling for water and oxygen filling.
Four different working methods, isoperibolic, dynamic, manual, time controlled makes possible an ideal adjustment of different operating tasks.
Clear and easily explained display which is simply to use .
With an external power pack, "world tension useable" from 100 - 240 V AC, 50/60 Hz. The operating voltage of the calorimeter is 24 V DC low- voltage.
Friendly in aftersales
Manual ( teaching mode): ignition and end of the measurement will be done by the operator himself; the temperature increase will be indicated at the display each minute.
All calculations have to be done manually.
At the other three modes ignition and calculation of the gross calorific value will be done automatically.
The gross calorific value will be shown on the display. Acid corrections and calculations of the net calorific value have to be done manually.
The modes have different measuring times:
Isoperibolic: approx: 17 min.
Dynamic : approx. 8 min
Manual : approx. 17 min
(depend on the operator)
Time controlled : 14 min
The decomposition vessel can be equiped in to use an combustible crucibles C 14
(accessory C 5010.4 attachment is neessary)
User-friendly software C 6040 Calwin for controlling the calorimeter and administration of measuring data (asseccory). Transfer of the datas to Excel or Word are possible
Up to eight IKA measuring cells can be controlled by a single PC, using a multiserial plug in card PCI 8.2 (accessory)
Accessories – C 200
The C 200 auto package allows operating the C 200 with a completely automated water cycle. This results in ease of handling and saves valuable time especially for laboratories with a low number of analyses. The water circulates in a closed loop and is kept at a constant temperature by using a recirculating chiller. This leads to shorter preparation time for each experiment and even better reproducible results.
The scope of delivery includes:
C 200 calorimeter measuring cell
C 5010 decomposition vessel
C 248 oxygen filling station
RC 2 basic recirculating chiller
C 200.RC hose set
Consumables for calibration and installation
The semi-automated and conforming to standards combustion calorimeter determines the gross calorific value of liquid and solid samples. So far it has mainly been used for teaching and training purposes at technical schools and universities. Due to the automated water handling it is now also suitable for industrial laboratories with low number of analyses.
Four different operation modes enable the user to control the measuring times according to individual requirements:
Isoperibol: approx: 17 min.
Dynamic : approx. 8 min
Manual : approx. 17 min (depends on the operator)
Time controlled : 14 min
Measurements are possible according to e.g. DIN 51900, ISO 1928, ASTM D240, ASTM D4809, ASTM D5865, ASTM D1989, ASTM D5468, ASTM E711.
The software C 6040 Calwin controls the unit and monitors the measurement of the samples. Additionally, collected data can be exported to e.g. Excel, Word, SQL and LIMS for further analysis. It is possible to operate several calorimeters with one PC. A PC is not part of the scope of delivery and needs to be provided by the operator. Calwin is sold separately.
Accessories – C 200 auto
C 6000 isoperibol Package 2/10
The C 6000 isoperibol oxygen bomb calorimeter combines modern technology, variability and automation in one instrument. It operates according to all bomb calorimeter standards, such as e.g. the DIN, ISO, ASTM, GOST and GB. The operator can choose between three different starting temperatures 22 °C, 25 °C, 30 °C in each measuring mode. Due to the new design of the decomposition vessel the measurement time could be reduced. Due to the variety of different interfaces for PC, printer (Ethernet, serial and USB), balance and USB Stick this unit is easily adaptable to the customer’s specific application needs. Further adaption to data management and LIMS is possible with our calorimeter software C 6040 Calwin (Accessory).
Measuring modes:
- isoperibol
- dynamic
Features:
- Automatic ignition and ignition energy determination
- Automatic water filling and draining
- Automatic oxygen filling, venting and flushing
- RFID technology for automatic decomposition vessel identification
- New design of the decomposition vessel allowing easier and faster sample preparation
- Easy and convenient capacitive touch screen operation
- Control chart view and correction calculation of globally used standards
- Ethernet interface to connect a network printer
- USB interface allowing easy data management and software updates
The C 6000 isoperibol Package 2/10 consists of:
- C 6000 isoperibol
- C 6010 decomposition vessel, standard
-
Accessories – C 6000 isoperibol Package 2/10
PRICEUSD 3,154.00
PRICEUSD 71.00
PRICEUSD 4,005.00
PRICEUSD 8,009.00
PRICEUSD 1,742.00
PRICEUSD 3,288.00
PRICEUSD 346.00
PRICEUSD 151.00
PRICEUSD 1,858.00
PRICEUSD 4,599.00
PRICEUSD 6,574.00
PRICEUSD 4,548.00
PRICEUSD 260.00
PRICEUSD 328.00
PRICEUSD 9,518.00
PRICEUSD 601.00
The C 1 static jacket oxygen bomb calorimeter represents a giant leap forward in calorimeter technology by featuring a high degree of automation in a compact design; the smallest calorimeter footprint available.
It operates according to DIN 51900 and ISO 1928. The temperature readings are analyzed according to the classical isoperibol method of Regnault Pfaundler.
The traditionally known, comparably heavy screw threaded decomposition vessel, has been replaced by a light and easily attachable combustion chamber.
Due to the variety of different interfaces (PC, balance, printer) this unit is easily adaptable depending on the customer’s specific application needs. Further adaption to data management and LIMS is possible with our calorimeter software C 6040 Calwin (Accessory).
The C 1 Package 1/10 contains the C 1 Calorimeter (inclusive standard combustion chamber C 1.10) and the cooling water supply unit RC 2 basic.
The unit contains all parts necessary to set up the unit. We also supply wear parts and consumables for the first approximately 500 experiments including 25 calibrations. The C 1.10 combsution chamber is equipped with the C 5010.5 large crucible holder and C 6 large quartz crucible.
Accessories – C 1 Package 1/10
The quartz digestion vessel enables the digestion process to be visible;
Initiative wireless remote video monitoring system, together with quartz vessels, makes the reaction be seen clearly at a glance. Pictures and videos can be taken during the entire process;
500 ml ultra-large digestion vessel meets the special requirements for the digestion of samples of up to 10 grams.
The drying rotor aides in the drying process of samples,
Sineo’s patented safety bolt design eliminates the need for explosion-proof membranes and other costly consumables.
The Aerospace composite fiber outer vessel ensures the highest level of vessel security.
Large 65L stainless steal chamber and dual magnetron structure, is designed for high energy and uniform microwave field.
With over 20 years of experience in the industry Sineo is known asa innovation leader with numerous patents.
Our Latest microwave system (The MDS-15)is the culmination of over 20 years of refinement. The MDS-15 is a high-throughput, multi-functional closed microwave sample preparation workstation with the latest technology and a lifetime warranty on the core component. Versatility: The MDS-15 is a versatile microwave which can handle the routine work, and more complicated and demanding samples in your prep rack with a wide variety of vessels to choose from. Safety is priority number one! At Sineo we put safety at the top priority, which is why we have painstakingly designed every aspect of our microwave system with the highest level of security measures, such as the use of aerospace composite fiber vessel sleeves, and our patented Safety Bolt. Efficient by design: MDS-15 applies high-energy uniform microwave field, it delivers a rapid digestion with a quick 20 minute cool down time. Sineo has incorporated the latest technology of material design while engineering a very safe, durable and easy to use microwave.
Functional vessels for your various application needs
Conventional digestion:
With 16 high-throughput GP-100 digestion vessel set, MDS-15can work for long time digestion at ultra high temperature. It meets the requirements for most of the digestion tasks; the new 8 QZ-100 quartz closed vessel set dramaticallyimproves the digestion capability and visibility, even the most demanding materials could be successfully digested. With remote Wi-Fi video monitoring system for quartz vessel, the whole process canbe observed, pictures and videos are available duringthe entire process.
Ultra-high sample amounts digestion:
LV-500 digestion vessel carousel enables eight 500ml ultra large vessels to digest simultaneously, upgrading the sample amount to an unparalleled level of 10 gram. With magnetic stirring feature, sample digestion could be done more quickly and thoroughly. Innovative Safety Bolt design ensures the combination of vertical & quantitative pressure relief and complete digestion. The digestion tasks of high sample amount thus could be accomplished.
Sample drying:
The F-DRY drying rotor supports rapid and uniform microwave drying, the sample drying time is only a quarter that of traditional method, it can also prevent sample contamination and carbonation. There’s no need of any modification to the main machine to complete the drying task.
Microwave extraction, microwave Kjeldahl Nitrogen Determination, etc:
Sineo’s application engineers have developed the application methods for microwave extraction, microwave Kjeldahl nitrogen determination, etc. Our technical support is at your service all the time.
The outer vessel of MDS-15 exclusively made by ultra strength aerospace composite fiber is invincible in anti-explosion, and its performance indicators such as corrosion resistance, high temperature/impact/pressure resistance are far better than that of the widely used modified PEEK engineering plastics vessel (this material is fusible at high temperature,fragile at high pressure and explosive by chemical corrosion)，fundamentally eliminating safety risks to operator in use.
The Halo SB-10 single beam spectrophotometer combines exceptional value with precision spectrophotometry in an uncomplicated package.
Spectral Features
The Halo SB-10 can achieve a 2 nm spectral band pass for superior spectra and peak resolution with its single beam optics. Other specifications include a wavelength accuracy of 
0.5nm, baseline stability 0.002Abs/hr (500nm) and stray light 
0.05%T (220nm NaI, 340nm NaNO2).
Photometry
Perform quantitative analyses in either absorbance or transmittance modes and in single wavelengths within a range of 190-1100nm.
Dual Lamp Advantage
By virtue of the halogen tungsten and deuterium lamps typically found in higher end, analytical spectrophotometers the Halo SB-10s wavelength range is an impressive 190nm - 1,100nm. A dual lamp system also results in higher accuracy than corresponding xenon lamps. Lamp switching is automatic (by default at 340nm) and both lamps are long life.
Others Features
Validation FunctionsStand alone or (Optional) PC Operation4-Sample Cuvette Holder
